Determination of Total Iodine in Food Samples Using Inductively Coupled PlasmaMass Spectrometry
نویسندگان
چکیده
منابع مشابه
Improved measurement of iodine in food samples using inductively coupled plasma isotope dilution mass spectrometry.
A new ICP-MS method for the determination of iodine in food samples is presented. The method makes use of a new miniature cyclonic spray chamber and a concentric glass nebulizer that is designed for low sample uptakes and is operated in a self-aspirating mode. As a consequence the wash-out was accelerated over conventional systems. This configuration allows the direct determination of iodine in...
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Iodine determination in food samples was performed by inductively coupled plasma mass spectrometry (ICP-MS) after digestion by microwave-induced combustion (MIC). Sample masses up to 500 mg of bovine liver, corn starch, milk powder, or wheat flour were completely combusted using the MIC system. Ammonium nitrate (6 mol l(-1) solution, 50 μl) was used as an aid for ignition and vessels were charg...
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BACKGROUND Honey contains a complex mixture of carbohydrates and other minor substances. Elements are minor constituents of honey that may threaten the human health in excess concentrations. So, determining the metals in honey helps its quality control as a food product. The aim of this study was to determine the concentrations of some metals in Iranian honey. METHODS This study was performed...
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In the present study a cloud-point extraction process using non-ionic surfactant Triton X-114 for selective extraction of gallium from aqueous solutions was developed. The method is based on the complex formation of Ga (III) with N, N′ -bis (salycilidene)-1, 2-phenylenediamine (salophen) as a chelating agent in buffer media of pH 5. After phase separation and dilution of the surfactant-rich pha...
متن کاملDirect determination of urinary iodine by inductively coupled plasma mass spectrometry using isotope dilution with iodine-129.
An inductively coupled mass spectrometric method was developed for the direct determination of iodine in urine. The application of isotope dilution analysis with added 129I offers new possibilities for automatic and accurate determinations. The sample preparation consists of dilution with an ammonia solution containing 129I. The validation was made by comparison with the results obtained in ano...
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ژورنال
عنوان ژورنال: Journal of AOAC INTERNATIONAL
سال: 2009
ISSN: 1060-3271,1944-7922
DOI: 10.1093/jaoac/92.6.1720